HORIZONS
REGULATORY AFFAIRS UPDATE
Fourteenth Issue
Fall 2001

In the six months since the publication of the last edition of HORIZONS, two important issues have developed into growing customer concerns. These issues could affect our business in a number of ways, so we are devoting the first half of this edition to their review. The two topics are aromatic amines and endocrine disrupters. In the second half of the publication, we will address reactions to these issues in light of the current state of analytical technology.

While these issues have their origin in Europe, the growing interest of our customers in the U.S. is an indicator of the global nature of both emerging regulatory concerns and the end user companies we ultimately serve.

AROMATIC AMINES
An article published in a Danish business magazine [Børsens Nyhedsmagasin] in August 2001, and subsequently picked up by the media in other countries, announced the presence of aromatic amines in flexible food packaging. These suspected carcinogens were said to be present in food packaging at many times the safe limit. (The analytical work supporting this conclusion was sponsored by the magazine and is presently the subject of some controversy.)

The issue in the media does not directly concern printing ink. Only the two-part adhesive used in the manufacture of laminated food packaging was implicated as the source of the aromatic amines. Concerns revolve around unreacted toluene diisocyanate (TDI) that can form the corresponding amine in undercured laminating adhesives.

In ink formulating, aromatic amines are not intentional raw material ingredients. Still, many commercial printing inks are formulated with polyurethane resins that often utilize aromatic isocyanates in their synthesis. These isocyanates react during the manufacturing process to produce the polymer. At the part-per-billion level, residual isocyanate may be detectable in the resin. Printing inks containing these types of polyurethane resins have not been implicated as a danger by any scientific group or regulatory agency at this time. However, ink makers are being questioned by their customers who want guarantees that there is no TDI in the ink.

ENDOCRINE DISRUPTERS
We turn now to a much broader array of chemicals that fall into a new general definition related to their potential activity in the human body. They are collectively called endocrine disrupters. The biological role of the endocrine system is extremely complex, and involves the immune and nervous systems, as well as sexual development. Endocrine disrupters are chemicals that may mimic or interfere with the hormones in the body.

The development and functioning of the body depends on a complex interaction of chemicals, in which everything must happen at the right time. Three crucial functions in the human body are the immune system, the hormonal system and the nervous system. Many of the interactions within and between these systems depend on fairly simple chemicals, all of which are potential targets for imitation by man-made chemicals.

The complexities of the endocrine system make it very difficult to predict the influence of chemicals on the body. There is evidence that disrupters affect some forms of animal life, but their effect in humans is a matter of long-standing debate. While it is easy to detect abnormalities in some parts of the body, detecting changes in the endocrine system is much harder. This is one of the reasons that providing proof of harm to any of these systems is difficult, unless the harm is very substantial.

There are at present close to 600 chemical compounds that have evidenced varying degrees of endocrine disrupting behavior. Disrupters include many common materials that are utilized in industry, such as plasticizers, antioxidants, detergents and polymer catalysts. In particular, there have been questions raised in Europe about the use of phthalate esters, antioxidants such as BHA, alkylphenols, bisphenol A, and tributyl tin to name a few.

REACTING TO THE ISSUES
We need to address the implications of these issues in light of the current state of analytical technology. The most common reaction by customers and end users is to bar the offending chemicals from all converted products or inks. (This is the basis for historical "negative" lists of chemicals.) However, even though these chemicals are not direct raw material ingredients in a formulation, there are still three problems with that approach.

First, the common ability to measure chemical species in the parts-per-billion range makes it difficult to define "none" or to rely on a changing definition over time. Second, it is difficult to obtain knowledge of contaminant levels of offending chemicals in the long supply chains typical to formulating industries. Third, as the list of "negative" materials grows, it is unlikely that they can all simply be removed from commerce.

What must ultimately replace negative lists is a process based on risk assessment. This concept often has difficulty being accepted, but has proved its worth in the past. Using risk assessment, both government and industry have quantified exposure to residual or background concentrations of chemicals. The control relies on how and how much of a chemical will be bioavailable.

Further, the models must account for how much of a material can become part of the daily intake of nutrients (food and drink) to the body. This quantity is expressed in maximum intakes in milli or micro grams per day. The intake is based on the risk modeling of sources further and further away from the actual food we eat. An example of differing potentials needs to be considered for the ink on a package, the amount of plasticizer in the printed film, the amount of catalyst in a polymer that is the film-former in the ink, etc.

The process seems complicated at first view, but such models are commonly used by the Food and Drug Administration (FDA) to evaluate the threshold of regulation for additives to food. We believe this should be the subject of exploration between the elements of our mutual supply chain from ink raw material suppliers to end users. Rather than banning certain chemicals outright, assessing risk of exposure could allow the continued safe use of the broadest range of our industry’s most common – and valuable – raw materials.